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2.3-二氯吡啶的運(yùn)用大大減少了萃取劑的運(yùn)用

作者：發(fā)布時間：2017-6-10 15:23:36 人氣：

2.3-二氯吡啶的運(yùn)用大大減少了萃取劑的運(yùn)用
華中師范大學(xué) 碩士學(xué)位論文 2，3-二氯吡啶組成技術(shù)研究名字：馮忖請求學(xué)位級別：碩士專業(yè)：農(nóng)藥學(xué) 輔導(dǎo)老師：楊光富;毛春暉座機(jī)電話號碼碩士學(xué)位論文 ⑨MASTER’STHESIS 摘要 2，3．二氯吡啶是新型殺蟲劑氯蟲苯甲酰胺的關(guān)鍵中-心體。氯蟲苯甲酰胺酰胺殺蟲劑，該殺蟲劑構(gòu)造新穎，作用方式共同，對鱗翅目害蟲有特-效，對哺乳動物的毒性很低，而且其具有高-效、廣-譜、與現(xiàn)有農(nóng)藥無交互抗性等優(yōu)點(diǎn)，適合于抗性管理與害蟲歸納。在文獻(xiàn)調(diào)研的基礎(chǔ)上，咱們對比了2，3．二氯吡啶的各種組成道路，斷定了以煙酰胺為開始質(zhì)料，通過霍夫曼酰胺降解，再通過氯化反響、重氮化和Sandmeyer反應(yīng)獲得2。3．二氯吡啶的技術(shù)道路，收率以煙酰胺計(jì)達(dá)62％，含量達(dá)99％。還探究了以3．氨基吡啶為質(zhì)料，中-心產(chǎn)物不純化，一鍋法組成2，3．二氯吡啶的道路，簡化了操作，易于完成工業(yè)化，收率以3一氨基吡啶計(jì)達(dá)66％，含量達(dá)98％以上。這篇文章對2，3．二氯毗啶的組成技術(shù)過程中每一步反響都做了大量探究與條件實(shí) 驗(yàn)，得出了優(yōu)惠反響條件：在3．氨基吡啶的組成中，學(xué)習(xí)別的文獻(xiàn)的辦法，篩選了幾種酰胺水解壓制劑而且斷定了其合適濃度，提高了反響的選擇性與收率；在3．氨基吡啶的后處理階段，針對3．氨基吡啶在水中溶解度較大，規(guī)劃搭建了一套接連回流萃取裝置，大大減少了萃取劑的運(yùn)用，通過改善后的技術(shù)收率到達(dá)90％；在2．氯一3．氨基吡啶的組成中，優(yōu)化各個反響條件減少了過度氯化的

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